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Table 2 Optimization of catalyst loading in preparation of 2b

From: A rapid, convenient, solventless green approach for the synthesis of oximes using grindstone chemistry

Entry

Catalyst loading (mol%)

Time

Yield (%)

1

No

2 h

15

2

20

30 min

48

3

30

30 min

57

4

40

30 min

70

5

50

15 min

90

6

60

2 min

96

7

70

2 mins

96