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Table 2 Synthesis of symmetrical bis(benzhydryl)ethers using p -TsCl as reagent under solvent-free conditions following Figure 2

From: Facile synthesis of symmetrical bis(benzhydryl)ethers using p-toluenesulfonyl chloride under solvent-free conditions

Entry

Alcohol

Product

Time (min)

Yield (%) a

Melting point (°C)

     

Found

Reported

1

15

86

106 to 107

105 to 107 [34]

2

15

89

Semisolid

Present work

3

10

85

Semisolid

Present work

4

10

92

Semisolid

Present work

5

10

88

125 to 127

126 to 127 [34, 35]

6

8

91

88 to 90

Present work

7

12

90

Semisolid

Present work

  1. aIsolated yield.