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Table 2 Synthesis of symmetrical bis(benzhydryl)ethers using p -TsCl as reagent under solvent-free conditions following Figure 2

From: Facile synthesis of symmetrical bis(benzhydryl)ethers using p-toluenesulfonyl chloride under solvent-free conditions

Entry Alcohol Product Time (min) Yield (%) a Melting point (°C)
      Found Reported
1 15 86 106 to 107 105 to 107 [34]
2 15 89 Semisolid Present work
3 10 85 Semisolid Present work
4 10 92 Semisolid Present work
5 10 88 125 to 127 126 to 127 [34, 35]
6 8 91 88 to 90 Present work
7 12 90 Semisolid Present work
  1. aIsolated yield.